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Principles and Applications of Asymmetric Synthesis | Publisher: Wiley-Interscience; 1 edition (February 7, 2001) | ISBN: 0471400270 | Pages: 536 | PDF | 22.65 MB

Asymmetric synthesis remains a challenge to practicing scientists as the need for enantiomerically pure or enriched compounds continues to increase. Over the last decade, a large amount of literature has been published in this field. Principles and Applications of Asymmetric Synthesis consolidates and evaluates the most useful methodologies into a one-volume resource for the convenience of practicing scientists and students.

Authored by internationally renowned scientists in the field, this reliable reference covers more than 450 reactions and includes important stoichiometric as well as catalytic asymmetric reactions. The first chapter reviews the basic principles, common nomenclature, and analytical methods, and the remainder of the book is organized according to reaction type. The text examines such topics as:

* Carbon-carbon bond formations involving carbonyls, enamines, imines, and enolates
* Asymmetric C-O bond formations including epoxidation, dihydroxylation, and aminohydroxylation
* Asymmetric synthesis using the Diels-Alder reaction and other cyclizations
* Applications to the total synthesis of natural products
* Use of enzymes in asymmetric synthesis

Practicing chemists in the pharmaceutical, fine chemical, and agricultural professions as well as graduate students will find that Principles and Applications of Asymmetric Synthesis affords comprehensive and current coverage.


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Lin and colleagues Yue-Ming Li and Albert S. C. Chan (all chemical technology, Hong Kong Polytechnic U.) consolidate and evaluate the most useful methodologies for producing enantiomerically pure or enriched compounds. After reviewing the basic principles, common nomenclature, and analytical methods, they describe over 450 reactions, among them stoichiometric and catalytic asymmetric. Their topics include aldol and related reactions, asymmetric oxidations, catalytic hydrogenation and other reduction reactions, and applying asymmetric reactions in synthesizing natural products. Practicing chemists in the pharmaceutical, fine chemical, and agriculture industries are the target readers.

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Chemistry: An Industry-Based Laboratory Manual | Publisher: CRC Press | pages: 248 | 2000 | ISBN: 1566703468 | PDF | 11,7 mb

Have you ever had a discussion with an industrial chemist about the job? Have you ever shadowed a chemist or chemical technician in an industrial or government laboratory for a day? If you have done these things, you were likely surprised at how foreign the language seemed or startled at how unfamiliar the surroundings were. Was there any talk of the quantum mechanical model of the atom? No. Was there any activity relating to Molecular Orbital Theory of bonding? No. Was the lab a large room with six 12-foot lab benches capable of accommodating up to two dozen chemists? No, not usually.Unless you took an "industry based" chemistry course, you probably came away from this experience with the thought "Why don't textbooks and lab manuals do a better job of communicating what real-world chemists do?" Chemistry: An Industry-Based Laboratory Manual does just that. It covers laboratory safety, record-keeping, control charts, certified reference materials, and much more. "Who uses this stuff anyway?" you may ask. Chemistry: An Industry-Based Laboratory Manual supplies the answer. It features applications of basic chemistry concepts to the real-world work of chemistry professionals. It brings real-world examples to laboratory experiences and covers voluntary industry standards for laboratory workers in the chemical process industries. It places a strong emphasis on the real work of chemistry professionals.


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Review
I would recommend this as a reference text and a source of ideas for instructors…I do envy the energy and imagination that John Kenkel shows in this text.
-Physical Sciences Educational Reviews Volume 6, Issue 1 June 2005
…well-organized, well-researched lab manual…impressively effective and comprehensive…I find this to be an excellent lab manual for training potential chemistry-based laboratory technicians. It is apparent that a lot of thought, effort, and expertise went into producing a lab manual that students and teachers alike can appreciate. Buy it! You'll like it!
-Sue Ballard, in Journal of Chemical Education, Vol. 78, No. 2

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Ion-Radical Organic Chemistry: Principles and Applications, Second Edition | CRC | 2008 | ISBN: 0849390680 | 672 pages | PDF |

Consolidating knowledge from a number of disciplines, Ion-Radical Organic Chemistry: Principles and Applications, Second Edition presents the recent changes that have occurred in the field since the publication of the first edition in 2003.

This volume examines the formation, transformation, and application of ion-radicals in typical conditions of organic synthesis. Avoiding complex mathematics, the author explains the principles of ion-radical organic chemistry and presents an overview of organic ion-radical reactions. He reviews methods of determining ion-radical mechanisms and controlling ion-radical reactions. Wherever applicable, the text addresses issues relating to ecology and biomedical concerns as well as inorganic participants of the ion-radical organic reactions.

After reviewing the nature of organic ion-radicals and their ground-state electronic structure, the book discusses their formation, the relationship between electronic structure and reactivity, mechanism and regulation of reactions, stereochemical aspects, synthetic opportunities, and practical applications. Additional topics include electronic and opto-electronic devices, organic magnets and conductors, lubricants, other materials, and reactions of industrial or biomedical importance.

The book concludes by providing an outlook on possible future development in this field. Researchers and practitioners engaged in active work on synthetic or mechanistic organic chemistry and its practical applications will find this text to be invaluable in both its scope and its depth.


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Recoverable and Recyclable Catalysts Wiley | 2009 | ISBN: 0470681950 | 500 pages | PDF |

There is continued pressure on chemical and pharmaceutical industries to reduce chemical waste and improve the selectivity and efficiency of synthetic processes. The need to implement green chemistry principles is a driving force towards the development of recoverable and recyclable catalysts.

The design and synthesis of recoverable catalysts is a highly challenging interdisciplinary field combining chemistry, materials science engineering with economic and environmental objectives. Drawing on international research and highlighting recent developments, this book serves as a practical guide for both experts and newcomers to the field.

Topics covered include:

* An introduction to the principles of catalyst recovery and recycling
* Catalysts on insoluble and soluble support materials
* Thermomorphic catalysts, self-supported catalysts and perfluorous catalytic systems
* The development of reusable organic catalysts
* Continuous flow and membrane reactors

Each chapter combines principles with practical information on the synthesis of catalysts and strategies for catalyst recovery. The book concludes with a comparison of different catalytic systems, using case studies to illustrate the key features of each approach.

Recoverable and Recyclable Catalysts is a valuable reference source for academic researchers and professionals from a range of pharmaceutical and chemical industries, particularly those working in catalysis, organic synthesis and sustainable chemistry.


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The Nature of the Hydrogen Bond: Outline of a Comprehensive Hydrogen Bond Theory | Oxford University Press, USA | Pages: 304 | 2009-08-25 | ISBN 0199558965 | PDF |

Hydrogen bond (H-bond) effects are known: it makes sea water iquid, joins cellulose microfibrils in trees, shapes DNA nto genes and polypeptide chains into wool, hair, muscles or enzymes. Its true nature is less known and we may still wonder why O-H...O bond energies range from less than 1 to more than 30 kcal/mol without apparent reason. This H-bond puzzle is re-examined here from its very beginning and presented as an inclusive compilation of experimental H-bond energies and geometries.

New concepts emerge from this analysis: new classes of systematically strong H-bonds (CAHBs and RAHBs: charge- and resonance-assisted H-bonds); full H-bond classification in six classes (the six chemical leitmotifs); and assessment of the covalent nature of strong H-bonds. This leads to three distinct but inter-consistent models able to rationalize the H-bond and predict its strength, based on classical VB theory, matching of donor-acceptor acid-base parameters (PA or pKa), or shape of the H-bond proton-transfer pathway.

Applications survey a number of systems where strong H-bonds play an important functional role, namely drug-receptor binding, enzymatic catalysis, ion-transport through cell membranes, crystal design and molecular mechanisms of functional materials.


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Organic Synthesis with Enzymes in Non-Aqueous Media | Publisher: Wiley | 2008-04-11 | ISBN: 3527318461 | Pages: 328 | PDF |

Closing a gap in the literature, this comprehensive book examines and discusses different non-aqueous systems from organic solvents to ionic liquids for synthetic applications, thus opening the door to new successful methods for biocatalytic reactions. It gathers into one handy source the information otherwise widely spread throughout the literature, combining useful background information with a number of synthetic examples, including industrial scale processes for pharmaceutical and fine chemicals.

Extremely well structured, the text introduces the fundamentals of non-aqueous enzymology, before going on to new reaction media and synthetic applications using hydrolases and non-hydrolytic enzymes. The one-stop reference for everyone working in this hot field.

Dr. Giacomo Carrea joined the Italian National Research Council (CNR) in 1969 where presently he is Director of the Institute of Chemistry of Molecular Recognition. He has been working in such fields as enzyme catalysis in organic solvents, synthesis of fine chemicals catalyzed by hydrolases, dehydrogenases, peroxidases and monooxygenases, study of conformation of proteins and polypeptides and analytical applications of bioluminescent enzymes. He is a member of the Editorial Board of "Trends in Biotechnology" and "Biocatalysis and Biotransformation" and the author of about 220 publications in international peer reviewed journals.

Dr. Sergio Riva is a Senior Research Scientist at the Institute of the Chemistry of Molecular Recognition. He took his Laurea in Chemistry in 1983 and his Diploma di Specialita in Organic Synthesis in 1989. In 1987 he was at M.I.T. (USA) working with Prof. A. Klibanov. In 1993 he was awarded the Ciamician medal by the Organic Chemical Division of the Italian Chemical Society for his research activity in biocatalysis, presently documented by more than 150 publications reporting on the isolation and characterization of enzymes and on the synthetic exploitation of these biocatalysts.


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Fundamentals of Analytical Chemistry | Publisher: Brooks Cole | ISBN: 0030355230 | edition 2003 | DJVU | 992 pages | 31 mb

FUNDAMENTALS OF ANALYTICAL CHEMISTRY, EIGHTH EDITION is known for its readability combined with a systematic, rigorous approach that characterizes this classic text. Extensive coverage of the principles and practices of quantitative chemistry ensures suitability for chemistry majors. These award-winning authors include applications throughout industry, medicine, and all the sciences. The text's new design and wealth of new photographs by renowned chemistry photographer Charlie Winters serve to reinforce student learning through dynamic visuals. Reflecting the increased emphasis of spreadsheets as a tool in analytical chemistry, this new edition adds an additional chapter, new problems and a new supplement, EXCEL® APPLICATIONS FOR ANALYTICAL CHEMISTRY, that integrate this important aspect of the study of analytical chemistry into its already rich pedagogy. In addition, the INTERACTIVE ANALYTICAL CHEMISTRY CD-ROM, packaged FREE with every new text, enhances conceptual understanding through hands-on integrated multimedia interactivity.

This two-semester textbook introduces the principles, techniques, and laboratory skills that are used in modern chemical analysis. The included CD-ROM contains tutorials and guided simulations. The eighth edition adds chapters on sampling and calibration and the use of spreadsheets.


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Douglas A. Skoog was granted a B.S. in chemistry from Oregon State University and received his Ph.D. in analytical chemistry from the University of Illinois. The lead author of several best-selling texts, Dr. Skoog is the 1999 recipient of the American Chemical Society award in analytical chemistry, sponsored by the Fisher Scientific Company. That same year, he was named a Fellow of the American Association for the Advancement of Science. In 1993, he received the ACS Division of Analytical Chemistry Award for Excellence in Teaching. He is Professor Emeritus of Chemistry at Stanford University.

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Nanoscale Materials in Chemistry, Second Edition | Wiley | 2009-10-26 | ISBN: 0470222700 | 789 pages | PDF | 12,2 MB

A comprehensive reference on nanoscale materials chemistry—now revised and updated. This extensive text provides twenty-two revised chapters on the preparations, applications, and characterization as well as the environmental and toxicological aspects of nanoscale materials, with an emphasis on the chemistry component. This Second Edition contains core topics including:

* New synthetic methods for nanomaterials
* Nanostructured solids
* Organized two- and three-dimensional nanocrystals
* Nanotubes, ribbons, and sheets
* Nanocatalysts, sorbents, and energy applications
* Unique physical properties of nanomaterials
* Photochemistry of nanomaterials
* Biological and environmental aspects of nanomaterials

With input from top experts in the field, such as Bruce Dunn, Vicki Grassian, Warren Ford, and Chris Sorensen, among others, Nanoscale Materials in Chemistry presents a balanced survey of different topics in basic nanoparticle science, and includes helpful end-of-chapter questions and answers. Significantly expanded, the Second Edition remains a key text for understanding the fundamentals of nanoscale materials chemistry and a reliable resource for scientists and researchers.


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KENNETH J. KLABUNDE, PhD, is the University Distinguished Professor at Kansas State University. His research focuses on materials science, nanoscale particles, magnetic properties of nanoscale iron particles, adsorption properties of nanoscale metal oxide properties, and organometallic chemistry. He is the editor of the first edition of Nanoscale Materials in Chemistry, also published by Wiley.

RYAN M. RICHARDS, PhD, is Associate Professor of Chemistry at the Colorado School of Mines. His research interests include nanoparticle preparations and characterization, as well as heterogeneous and enantioselective catalysis.

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Principles of General Chemistry | Martin Silberberg | August 23, 2006 | ISBN: 007330171X | English | 896 pages | HQ PDF | 114 MB

Silberberg’s Principles of General Chemistry offers students the same authoritative topic coverage as his 4th edition textbook while appealing to today’s efficiency-minded and value-conscious instructors and students. Principles allows for succinct coverage of content with minimal emphasis on pedagogic learning aids. This new approach offers a more straightforward approach to learning the core principles without sacrificing depth, clarity, or rigor.

Martin S. Silberberg received his B.S. in chemistry from the City University of New York in 1966 and his Ph.D. in chemistry from the University of Oklahoma, in 1971. He then accepted a research position at the Albert Einstein College of Medicine, where he studied the chemical nature of neurotransmission and Parkinson's disease. In 1977, Dr. Silberberg joined the faculty of Simon's Rock College of Bard (Massachusetts), a liberal arts college known for its excellence in teaching small classes of highly motivated students. As Head of the Natural Sciences Major and Director of Premedical Studies, he taught courses in general chemistry, organic chemistry, biochemistry, and nonmajors chemistry. The close student contact afforded him insights into how students learn chemistry, where they have difficulties, and what strategies can help them succeed. In 1983, Dr. Silberberg decided to apply these insights in a broader context and established a text writing and editing company. Before writing his own text, he worked on chemistry, biochemistry, and physics texts for several major college publishers. He resides with his wife and child in Massachusetts. For relaxation, he cooks, sings, and walks in the woods.


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Principles of General Chemistry | Martin Silberberg | August 23, 2006 | ISBN: 007330171X | English | 896 pages | HQ PDF | 114 MB

Silberberg’s Principles of General Chemistry offers students the same authoritative topic coverage as his 4th edition textbook while appealing to today’s efficiency-minded and value-conscious instructors and students. Principles allows for succinct coverage of content with minimal emphasis on pedagogic learning aids. This new approach offers a more straightforward approach to learning the core principles without sacrificing depth, clarity, or rigor.

Martin S. Silberberg received his B.S. in chemistry from the City University of New York in 1966 and his Ph.D. in chemistry from the University of Oklahoma, in 1971. He then accepted a research position at the Albert Einstein College of Medicine, where he studied the chemical nature of neurotransmission and Parkinson's disease. In 1977, Dr. Silberberg joined the faculty of Simon's Rock College of Bard (Massachusetts), a liberal arts college known for its excellence in teaching small classes of highly motivated students. As Head of the Natural Sciences Major and Director of Premedical Studies, he taught courses in general chemistry, organic chemistry, biochemistry, and nonmajors chemistry. The close student contact afforded him insights into how students learn chemistry, where they have difficulties, and what strategies can help them succeed. In 1983, Dr. Silberberg decided to apply these insights in a broader context and established a text writing and editing company. Before writing his own text, he worked on chemistry, biochemistry, and physics texts for several major college publishers. He resides with his wife and child in Massachusetts. For relaxation, he cooks, sings, and walks in the woods.


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